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Hydrogen

Atomic Force Microscopy Measurements of PEM Fuel Cells Processes

Davidson, D. F., S. C. Ranganath, K. Y. Lam, M. Liaw, Z. Hong, and R. K. Hanson. “Ignition delay time measurements of normal alkanes and simple oxygenates.” Journal of Propulsion and Power (submitted, 2009).
Shen, Y., D. M. Barnett, and P. M. Pinsky. “Analytic perturbation solution to the capacitance system between a hyberboloidal tip and a rough surface.” Applied Physics Letters, Vol. 92, 134105, doi:10.1063/1.2906487 (2008).
Shen, Y., D. M. Barnett, and P. M. Pinsky. “Simulating and interpreting Kelvin probe force microscopy images on dielectrics with boundary integral equations.” Review of Scientific Instruments, Vol. 79, 023711, doi:10.1063/1.2885679 (2008).
Shen, Y., M. Lee, W. Lee, D. M. Barnett, P. M. Pinsky, and F. B. Prinz. “A resolution study for electrostatic force microscopy on bimetallic samples using the boundary element method.” Nanotechnology, Vol. 19, 035710, pp. 1-13, doi:10.1088/0957-4484/19/03/035710 (2008).
Shen, Y., D. M. Barnett, and P. M. Pinsky. “Modeling electrostatic force microscopy for conductive and dielectric samples using the boundary element method.” Eng. Anal. Bound. Elem., Vol. 32, No. 8, pp. 682-691, doi:10.1016/j.enganabound.2007.12.003 (2007).
Shen, Y., D. M. Barnett, and P. M. Pinsky. “Integral equation modeling of electrostatic interactions in atomic force microscopy.” In: Integral Methods in Science and Engineering: Techniques and Applications (C. Constanda and S. Potapenko eds.), Birkhäuser, Boston, pp. 237-246, doi:10.1007/978-0-8176-4671-4 (2007).
Shen, Y., D. M. Barnett and P. M. Pinsky. “Precise modeling of AFM tip-sample interactions: capacitance and capacitive force computations,” (in preparation, 2006).
Shen, Y., D. M. Barnett and P. M. Pinsky, “Topographics effects on charge measurements by electrostatic force microscopy,” (in preparation, 2006).

Biohydrogen Generation

Meshulam-Simon, G., Choo, A. D. and Spormann, A. M. Hydrogen metabolism in Shewanella oneidensis MR-1. Appl. Envir. Microbiol., 73, 1153-1165 2007

C-H Bonds in Carbon Nanotubes as an Energy Carrier

Rajasekaran, Srivats, Sarp Kaya, Toyli Anniyev, Hirohito Ogasawara, and Anders Nilsson. "Probing substrate effects in the carbon-projected band structure of graphene on Pt (111) through resonant inelastic x-ray scattering." Physical Review B 85, no. 4 (2012): 045419.
Rajasekaran, Srivats, Sarp Kaya, Frank Abild-Pedersen, Toyli Anniyev, Fan Yang, Dario Stacchiola, Hirohito Ogasawara, and Anders Nilsson. "Reversible graphene-metal contact through hydrogenation." Physical Review B 86, no. 7 (2012): 075417.
Diao, Shuo, Guosong Hong, Joshua T. Robinson, Liying Jiao, Alexander L. Antaris, Justin Zachary Wu, Charina L. Choi, and Hongjie Dai. "Chirality Enriched (12, 1) and (11, 3) Single-Walled Carbon Nanotubes for Biological Imaging." Journal of the American Chemical Society, 134 (41), 16971–16974 (2012).
Bhowmick, R., S. Rajasekaran, D. Friebel, C. Beasley, L. Jiao, H. Ogasawara, H. Dai, B. Clemens, and A. Nilsson. “Hydrogen Spillover in Pt-Single-Walled Carbon Nanotube Composites: Formation of Stable C−H Bonds,” J. Am. Chem. Soc. 133, 14, 5580–5586, doi:10.1021/ja200403m (2011).
Nikitin, A., Zhang, Z.Y., Nilsson, A. Energetics of C-H Bonds Formed at Single-Walled Carbon Nanotubes. Nano Lett. 9:4, 1301-1306 (2009).
howmick, R., S. Rajasekaran, D. Friebel, C. Beasley, L. Jiao, H. Ogasawara, H. Dai, B. Clemens, and A. Nilsson. “Hydrogen Spillover in Pt-Single-Walled Carbon Nanotube Composites: Formation of Stable C−H Bonds,” J. Am. Chem. Soc. 133, 14, 5580–5586, doi:10.1021/ja200403m (2011).
Nikitin, A., Z. Y. Zhang, and A. Nilsson. “Energetics of C-H bonds formed at single-walled carbon nanotubes". Nano Letters, Vol. 9, No. 4, pp. 1301-1306, doi:10.1021/n1802727h (2009).

Direct Solar BioHydrogen

Boyer M. E, J. A. Stapleton, J. M. Kuchenreuther, C. W. Wang, and J. R. Swartz. “Cell-free synthesis and maturation of [FeFe] hydrogenases.” Biotechnology and Bioengineering, Vol. 99, No. 1, pp. 59-67, doi:10.1002/bit.21511 (2007).
Boyer, M.E., Wang, C.-W., and Swartz, J.R., Simultaneous expression and maturation of the iron-sulfur protein ferredoxin in a cell-free system., Biotechnology and Bioengineering, 94:128-138 (2006)

Hydrogen Effects on Climate, Stratospheric Ozone, and Air Pollution

Jacobson, M. Z. “Effects of wind-powered hydrogen fuel cell vehicles on stratospheric ozone and global climate.” Geophys. Res. Lett., 35, L19803, doi:10.1029/2008GL035102 (2008).
Colella, W.C., Jacobson, M.Z. & Golden D.M. Switching to a U.S. Hydrogen Fuel Cell Vehicle Fleet: The Resultant Change in Emissions, Energy Use, and Greenhouse Gases. J. Power Sources. 150, 150-181, October 4 (2005)
Archer, C.L. & Jacobson, M.Z. Evaluation of Global Wind Power. J. Geophys. Res.-Atm. 110, doi:10.1029/2004JD005462 (2005)
Jacobson, M.Z. A Refined Method of Parameterizing Absorption Coefficients Among Multiple Gases Simultaneously From Line-By-Line Data. J. Atmos. Sci. 62, 506-517 (2005)
Jacobson, M.Z., Colella, W.C. & Golden, D.M. Cleaning the Air and Improving Health with Hydrogen Fuel Cell Vehicles. Science. 308, 1901-1905, June 24 (2005)
Jacobson, M.Z. A Solution to the Problem of Non-Equilibrium Acid/Base Gas-Particle Transfer at Long Time Step. Aerosol Sci. Technol. 39, 92-103 (2005)
Jacobson, M.Z. Studying Ocean Acidification with Conservative, Stable Numerical Schemes for Non-Equilibrium Air-Ocean Exchange and Ocean Equilibrium Chemistry. J. Geophys. Res. 110, doi:10.1029/2004JD005220 (2005)

Micro and Nano Scale Electrochemistry Applied to PEM Fuel Cells

O’Hayre, R., M. Lee, F. B. Prinz, and S. V. Kalinin. “Frequency dependent transport imaging by scanning probe microscopy .” In: Scanning Probe Microscopy: Electrical and Electrochemical Phenomena at the Nanoscale, Gruverman and S. V. Kalinin (Eds.), Springer Verlag, New York (2007).
Lee, M., W. Lee, and F. B. Prinz. “Topology artifact suppressed Kelvin probe microscopy.” Nanotechnology (Submitted, 2006).
O’Hayre, R., D. M. Barnett, and F. B. Prinz. “The triple phase boundary: A mathematical model and experimental investigations for fuel cells.” Journal of the Electrochemical Society, Vol. 152, No. 2, A439-A444, doi: 10.1149/1.1851054 (2005).
>Shen, Y., D. M. Barnett, and P. M. Pinsky, Modeling electrostatic force microscopy for conductive and dielectric samples using the boundary element method: Eng. Anal. Bound. Elem., accepted for publication, doi:10.1016/j.enganabound.2007.12.003.
Shen, Y., D. M. Barnett, and P. M. Pinsky, Analytic perturbation solution to the capacitance system between a hyberboloidal tip and a rough surface: Appl. Phys. Lett., 92, 134105, 2008.
Shen, Y., D. M. Barnett, and P. M. Pinsky, Simulating and interpreting Kelvin probe force microscopy images on dielectrics with boundary integral equations: Rev. Sci. Instrum., 79, 023711, 2008.
Shen, Y., M. Lee, W. Lee, D. M. Barnett, P. M. Pinsky, and F. B. Prinz, A resolution study for electrostatic force microscopy on bimetallic samples using the boundary element method: Nanotechnology, 19, 035710, 2008.
Shen, Y., D. M. Barnett, and P. M. Pinsky, Integral equation modeling of electrostatic interactions in atomic force microscopy. In: C. Constanda and S. Potapenko (eds.), Integral Methods in Science and Engineering: Techniques and Applications, Birkhäuser, Boston, 237-246, 2007.
O’Hayre, R. & Prinz, F.B. The Air/Platinum/Nafion Triple Phase Boundary: Characteristics, Scaling, and Implications for Fuel Cells. J. Electrochem. Soc. 151, A756 (2004)
O’Hayre, R., Feng, G., Nix, W.D. & Prinz, F.B. Quantitative Impedance Measurement Using Atomic Force Microscopy. J. App. Phys. 96:6, 3540-3549 (2004)
O’Hayre, R., Lee, M. & Prinz, F.B. Ionic and Electronic Impedance Imaging Using Atomic Force Microscopy. J. App. Phys. 95:12, 8382-8392 (2004)
O’Hayre, R. “Micro Scale Electrochemistry: Application to Fuel Cells.” PhD Thesis, Dept. of Materials Science and Engineering, Stanford University (2004).
Fasching, R., Y. Tao, S.J. Bai, K. Hammerick, L. Smith, R. Greco, and F. Prinz. “Next generation sensors for measuring ionic flux in live cells.” In: Nano Biology, L. Smith, F. Prinz, R. Greco, Ed., CRC, Boca Raton, (in press, 2004).

Monitoring of the Bioconversion Processes

Fasching, R., Tao, Y., Bai, S-J., Hammerick, K., Smith, L., Greco, R. & Prinz, F. Next Generation Sensors for Measuring Ionic Flux in Live Cells in Nanoscale Technology in Biology (eds Greco, R., Prinz, F. & Smith, L.) 55-72 (CRC Press, Boca Raton, 2005)
Hammerick, K., Ryu, W-H., Fasching, R., Bai, S-J., Smith, L., Greco, R. & Prinz, F. Synthesis of Cell Structures in Nanoscale Technology in Biology (eds Greco, R., Prinz, F. & Smith, L.) 73-102 (CRC Press, Boca Raton, 2005)
Fasching, R., Tao, Y. & Prinz, F.B. Cantilever Tip Probe Arrays for Simultaneous SECM and AFM Analysis. Sens. Actuators B: Chem. 108:1-2, 964-972 (July 2005)

Nanomaterials Engineering for Hydrogen Storage

Bhowmick, R., B. M. Clemens, and B. A. Cruden. “Parametric analysis of chirality families and diameter distributions in single-wall carbon nanotube production by the oating catalyst method.” Carbon, Vol. 46, No. 6, pp. 907-922, doi:10.1016/j.carbon.2008.02.020 (2008).
Nikitin, A. “Hydrogen Storage in Carboneous Materials Through the Formation of C-H Bonds.” PhD Thesis, Dept. of Applied Physics, Stanford University (2008).
Niktin, A., X. Li, Z. Zhang, H. Ogasawara, H. Dai and A. Nilsson. “Hydrogen storage in carbon nanotubes through the formation of stable C-H bonds.” Nano. Lett., Vol. 8, No. 1, 162-167, doi:10.1021/nl072325k (2008).
Nikitin, A., L. A. Naslund, Z. Zhang and A. Nilsson. “C-H bond formation at the graphite surface studied with core level spectroscopy.” Surface Science, Vol. 602, No. 14, pp. 2575-2580, doi:10.1016/j.susc.2008.06.012 (2008).
Nikitin, A., X. Li, Z. Zhang, D. Mann, H. Ogasawara, H. Dai, and A. Nilsson. “Hydrogen storage in carbon nanotubes through the formation of C-H bonds,” (to be submitted, 2008).
Lee, Y-W. “Hydrogen Storage Properties of Catalyst Metal-Doped Single-Walled Carbon Nanotubes.” PhD Dissertation and Thesis, Dept. of Materials Science and Engineering, Stanford University (2007).
Zhang Z. and K. Cho. “Ab initio study of hydrogen interaction with pure and nitrogen doped carbon nanotubes,” (submitted to Phys. Rev. Lett., 2006).
Zhang, Z., H. Liu, and K. Cho. “Ab initio study of hydrogen storage capability of single walled carbon nanotubes,” (to be submitted to Nano Lett, 2006)
Zhang, Z., B. Magyari-Kope, and K. J. Cho. “Ab initio study of Li3N for hydrogen storage: Hydrogenation and reconstruction of the surfaces,” (in preparation, 2006)
Zhang, Z. and K. J. Cho. “Ab initio study of nucleation and diffusion of small Pd clusters on CNT,” (in preparation, 2006).
Lee, Y-W., B. M. Clemens, and K. J. Gross, “Novel Sieverts’ type volumetric measurements of hydrogen storage properties for very small sample quantities.” J. Alloys and Compounds, Vol. 452, No. 2, pp. 410-413, doi:10.1016/j.jallcom.2006.11.014, (2008) (online, 2006).
Zhang, G., Qi, P., Wang, X., Lu, Y., Mann, D., Li, X., & Dai, H. Hydrogenation and Hydrocarbonation and Etching of Single-Walled Carbon Nanotubes. J. Am. Chem. Soc. 128, 6026-6027 (2006)
Nikitin, A., Ogasawara, H., Mann, D., Zhang, Z., Dai, H. & Nilsson, A. Hydrogenation of Single Wall Carbon Nanotubes. Phys. Rev. Lett. 95:22, 225507 (2005)
Zhang, G., Mann, D., Zhang, L., Javey, A., Li, Y., Yenilmez, E., Wang, Q., McVittie, J., Nishi, Y., Gibbons, J., & Dai, H. Ultra-High-Yield Growth of Vertical Single-Walled Carbon Nanotubes: Hidden Roles of Hydrogen and Oxygen. PNAS 102:45, 16141-16145 (2005)
Lee, Y-W., R. Deshpande, A. C. Dillon, M. J. Heben, H. Dai, and B. M. Clemens. “The role of metal catalyst in near ambient hydrogen adsorption on multi-walled nanotubes,” Mater. Res. Soc. Symp. Proc., Vol. 837 (2005).
Mann, D., N. Wong, S. Kam, X-W. Tang, Y. Li, D. Wang, Q. Wang, L. Zhang, R. Tu, Y-L. Chang, and H. Dai. “Wafer scale free-floating transferable films of single-walled carbon nanotubes,” (submitted, 2005).
Orenstein, D. “Beyond Theory: Engineers hope nanotechnology can make hydrogen economy real.” Faculty Research Highlight, School of Engineering Website

Nuclear Magnetic Resonance Studies of Ceramic Materials for Fuel Cells

Huang, H., C-H. Hsieh, N. Kim, J. F. Stebbins, and F. Prinz. ‘Structure, local environment, and ionic conduction in scandia stabilized zirconia.” Solid State Ionics, Vol. 179, No. 27-32, pp. 1442-1445, doi:10.1016/j.ssi.2008.02.061 (2008).
Kim, N., C-H. Hsieh, H. Huang, F. B. Prinz, and J. F. Stebbins. “High temperature 17O MAS NMR study of calcia, magnesia, scandia and yttria stabilized zirconia.” Solid State Ionics, Vol. 178, No. 27-28, pp. 1499-1506, doi:10.1016/j.ssi.2007.09.008 (2007).
Kim, N. and J. F. Stebbins. “Vacancy and cation distribution in yttria-doped ceria: An 89Y and 17O MAS NMR Study.” Chem. Materials, Vol. 19, No. 23, pp. 5742-5747, doi:0.1021/cm0715388 (2007).
Kim, N. and J. F. Stebbins. “Scandium molybdate-scandium tungstate solid solutions: high resolution 45Sc and 17O NMR constraints on cation disorder,” (in preparation, 2007).
Kim, N., C-F. Hsieh, and J. F. Stebbins. “Scandium coordination in solid oxides and stabilized zirconia: 45Sc NMR.” Chem. Materials, Vol. 18, No. 16, 3855-3859, doi:10.1021/cm060590l (2006).
Kim, N., C.-H. Hsieh, and J. F. Stebbins. “Oxygen site exchange and ionic conductivity in zirconias: a high-resolution, high-temperature NMR study,” (in preparation, 2006.
Hsieh, C.-H. “Solid-state NMR and x-ray studies of local coordination environment in the ZrO2-Sc2O3 system.” M.S. Report, Dept. of Materials Science and Engineering, Stanford University (2005).
Kim, N., C-H. Hsieh, and J. F. Stebbins. “Scandium-stabilized zirconia: high-resolution NMR assessment of cation ordering,” (in preparation, 2005).

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